DIONEX Ионный Хроматограф ICS-2100
- Details
- Parent Category: Каталог Продуктов
- Category: Хроматографическое Оборудование
The ICS-2100 system is the first Reagent-Free™ ion chromatography system with electrolytic sample preparation (RFIC-ESP™ system) and eluent generation (RFIC-EG™ system) capabilities designed to perform all types of electrolytically generated isocratic and gradient IC separations using conductivity detection. Microbore 2 mm columns and standard bore 4 mm columns are fully supported.
ICS-2100 System Demo Video
The ICS-2100 RFIC-ESP system now provides automation for many sample preparation techniques with multiple valving configurations and support for electrolytic sample preparation devices.
The ICS-2100 system provides high performance with unequalled ease-of-use when coupled with an AutoSuppression® device, such as the SRS® 300 suppressor. Chromeleon® software provides full control and digital data collection from a PC using simple USB connectivity.
Key Features:
- Automated eluent generation
- LCD front panel control
- Dual-piston pump
- Column heater
- Electrolytic suppression
- Digital conductivity detection
- Vacuum degas (option)
- Optional 6- or 10-port valve
- Optional RFIC-ESP water purifier
- USB connectivity, plug-n-play
- Electronic logbook and trending through virtual channels
Benefits:
- RFIC-ESP system accessories enable control of electrolytic sample preparation devices such as water purifiers and sample conditioners.
- Sample preparation capabilities extend the range of the instrument into areas, such as on-line filtration, matrix elimination, neutralization, and ultratrace analysis.
- Flexible flow rates support 2, 3, 4, and 5 mm column formats.
- Column heater provides day-to-day consistency, ensuring reproducibility and stability. Preheating of the eluent prior to the column maintains the column temperature set by the user. A transparent cover allows viewing of the column without temperature disruption.
Achieve Results without the Problems and Cost of Manual Eluent Preparation and Now Automate Sample Preparation
Reagent-Free systems convert deionized water into high-purity eluents on-line, eliminating the labor of eluent preparation. In addition to being fully integrated, the ICS-2100 ships fully preconfigured, factory plumbed, and tested for immediate startup and performance. You begin to collect data within hours of installation. The ICS-2100 performs all types of IC separations using conductivity detection. With a space-conserving small-footprint design, the ICS-2100 occupies minimal bench space yet provides easy access to all vital system components. A new, integrated auxiliary valve available as an option enables a wide range of automated sample preparation techniques including on-line filtration, matrix elimination, and automatic reduced-volume reinjection of samples. Save time and money!
| ICS-2100 Integrated Reagent-Free IC System Specifications | |
|---|---|
| Analytical Pump and Fluidics | |
| Type | Serial dual-reciprocating pistons, microprocessor-controlled constant stroke, variable speed |
| Construction | Chemically inert, metal-free PEEK™ pump heads and flow paths compatible with aqueous eluents of pH 0–14 and reversed-phase solvents |
| Pump Operating Pressure | 0–35 MPa (0–5000 psi) |
| Flow Rate Range | 0.00–5.00 mL/min without changing pump heads |
| Flow Precision | <0.1%, typically |
| Flow Accuracy | <0.1%, typically |
| Pressure Ripple | <1% at 13.8 MPa (2000 psi) and 1.0 mL/min |
| Eluent On-Off Valve | Standard |
| Piston Seal Wash | Dual-pump head, wash can be continuous when connected to rinse solution supply |
| Pressure Alarm Limits | Upper limit 0–35 MPa or 0–5000 psi in one unit (MPa or psi) increments; lower limit can be set up to one unit lower than upper limit |
| Vacuum Degas | Yes, optional, automatic control |
| Eluent Bottles | Polypropylene, up to 4 L volume |
| Eluent Bottle Pressure | Not required |
| Injection Valve | 6-port, 2-position Rheodyne valve, electrically activated |
| Columns Supported | 2, 3, 4, and 5 mm i.d., maximum length 250 mm analytical column with 50 mm guard column |
| Column Heater | Standard |
| Operating Temperature Range | 30–60 °C (86–140 °F); minimum 5 °C above the ambient temperature. Settable range is equal to working range. |
| Temperature Accuracy | ±0.5 °C at sensor; at 40 °C |
| Eluent Generation | Standard |
| Eluent Types | KOH, LiOH, NaOH K2CO3 K2CO3/KHCO3 MSA |
| Gradient Profiles | Option; Combination of unlimited number of linear, convex and concave positive and negative gradient profiles |
| Concentration Increments | 0.01 mM |
| Concentration Range | 0.1–100 mM (depending on eluent used) |
| Flow Rate | 0.1–3.0 mL/min |
| Maximum Operating Pressure | 21 MPa (3000 psi) |
| Maximum Solvent Concentration | Anions: 25% methanol Cations: no solvents |
| Auxiliary Power Supply | Standard |
| Current | Constant, 0–200 mA at up to 35 V |
| Alarms | Overvoltage and overcurrent alarms; linked to pump flow to protect devices from power on at zero flow |
| Auxiliary Valve (Optional) | One 6- or 10-port, 2 position high-pressure Rheodyne valve, fully inert PEEK construction, electrically activated. Field installable, integrated into instrument |
| Eluent Regeneration Support | Yes, with optional RFIC-ER™ Startup kit |
| Eluents | Carbonate and carbonate/bicarbonate combinations up to 20 mM MSA up to 34 mM |
| Flow Rates | 0.01–2.00 mL/min |
| Continuous Operation (4 L of eluent) | Up to 28 days or 2000 samples, typically |
| Always On/Always Ready Capable | Yes, standard feature |
| Remains Fully Calibrated for Extended Periods (<28 days) |
Yes, standard feature. Results are traceable to a single calibration |
| System Wellness | Consumables usage monitoring for predictive maintenance |
| Maximum Operating Pressure | 21 MPa (3000 psi) |
| Operating Temperature Range | 4–40 °C |
| Suppressors and Control | |
| Chemical Suppression | 2 mm and 4 mm anion and cation, membrane suppression bed type |
| Displacement Chemical Regeneration | 2 mm and 4 mm anion and cation, membrane suppression bed type |
| Electrolytic Suppression- Self Regenerating. | 2 mm and 4 mm anion and cation. Both membrane and MonoDisk™ suppression bed types available |
| Electrolytic Suppression- Self Regenerating with External Water Mode | 2 mm and 4 mm anion and cation. Both membrane and MonoDisk suppression bed types available |
| Current Control Range | SRS®: 4 mm, 0–300 mA in 1 mA increments 2 mm, 0–100 mA in 1 mA increments AES®: 0–150 mA in 1 mA increments CMD: 0–500 mA in 1 mA increments SRN: 0–500 mA in 1 mA increments |
| CMD: | 0–500 mA in 1 mA increments |
| Salt Converter | Available in 2 and 4 mm versions |
| AMMS-ICE | Available in 2 and 4 mm versions |
| Carbonic Acid Removal for Anions | Yes: ASRS® 300 plus CRD 200 for hydroxide eluents ASRS 300 with CRD 300 for carbonate eluents |
| Non-Suppressed Chromatography | Yes, supported |
| Suppressor Wear Parts | None; peristaltic pump and inline filters are not required |
| Suppression Capacity | Anion SRS 300 (4 mm): 200 µeq/min Cation SRS 300 (4 mm): 110 µeq/min Anion SRS 300 (2 mm): 50 µeq/min Cation SRS 300 (2 mm): 37.5 µeq/min Anion MMS™ 300 (4 mm): 150 µeq/min Cation MMS 300 (4 mm): 150 µeq/min Anion MMS 300 (2 mm): 37.5 µeq/min Cation MMS 300 (2 mm): 37.5 µeq/min Anion AES: 25 µeq/min Cation AES:25 µeq/min |
| Void Volumes | SRS 300 (4 mm): <50 µL SRS 300 (2 mm): <15 µL MMS 300 (4 mm): <50 µL MMS 300 (2 mm): <15 µL AMMS-ICE 300 (4 mm): <50 µL AMMS-ICE 300 (2 mm): <15 µL AES (Anion or Cation): <35 µL |
| Conductivity Detector Electronics and Flow Cell | |
| Type | Microprocessor-controlled digital signal processor |
| Cell Drive | 8 kHz square wave |
| Linearity | 1% up to 1 mS |
| Resolution | 0.00238 nS |
| Full-Scale Output Ranges | Digital signal range 0–15,000 µS Analog signal range 0–15,000 µS |
| Electronic Noise | ±0.1 nS when background conductivity is 0–150 µS/cm ±2 nS when background conductivity is 151–3200 µS/cm |
| Filter | Rise times from 0 to 10 s, user selectable |
| Temperature Compensation | Fixed at 1.7%/°C at cell temperature |
| Temperature Range | Ambient +7 °C; 30–55 °C |
| Cell Electrodes | Passivated 316 stainless steel. Compatible with MSA |
| Cell Body | Chemically inert polymeric material |
| Cell Volume | <1 µL |
| Heat Exchanger | Inert, tortuous-path for low axial dispersion |
| Maximum Cell Operating Pressure | 10 MPa (1500 psi) |
| Autosampler | |
| Automation Using Autosampler | Dionex AS-DV, AS, AS-HV, or third-party Autosamplers |
| Sequential/Simultaneous Injection | Yes, depending on autosampler capabilities |
| Automated Dilution | Yes, available with AS Autosampler |
| Dilution Factor, AS Autosampler | 1:1 to 1:1000 |
| Dilution Time, AS Autosample | 15 seconds with sample overlap |
| Inline Sample Degassing | Yes, optional with CRD 200/300 |
| Inline Filtration | Yes, AS-DV Autosampler or inline filter |
| High Automation Flexibility | Conditionals using Chromeleon® software and post run features |
| System Software and Control | |
| Software | Chromeleon Chromatography Data System software, supports Microsoft Windows® XP, or Vista |
| Automated Procedure Wizards | Yes, standard feature |
| Data Trending Plots | Yes, numerical device parameters can be plotted |
| Virtual Column Simulator | Yes; evaluation mode standard, isocratic and gradient optional |
| Application Templates | Yes, standard feature |
| Multivendor Automation Support of 3rd Party Instruments | Yes, fully controls over 300 different instruments from more than 30 manufacturers, including GC, HPLC, and MS |
| 3-D Software for PDA and MS | Yes, optional |
| Customizable System Control Panels | Yes, standard feature |
| System Status Virtual Channel | Yes, standard feature |
| Power Failure Protection | Yes, standard feature |
| Sequential Injection | Yes, standard feature for independent dual system analysis |
| System Trigger Commands and Conditionals | Yes, standard feature |
| Daily Audit Trail | Yes, standard feature |
| Sample Audit Trail | Yes, standard feature |
| Multiple Network Control and Network Failure Protection | Yes, optional |
| System Calibration Storage | Yes, factory, present and previous. Completely user selectable |
| Customized Reporting | Yes, standard feature with unlimited report workbooks |
| Control Modes | Full control through front panel and Chromeleon software; alternative control through TTL or relay closures; two relay outputs, two TTL outputs, four programmable inputs |
| Semi Automated System Qualification | Yes, automated IQ/OQ/PQ procedures produce detailed, comprehensive qualification reports using minimal operator time |
| USB Communication Protocol | One input; one built-in two-port USB hub |
| Physical Specifications | |
| Dimensions (h × w × d) | 56.1 cm × 22.4 cm × 53.3 cm (22.1 in × 8.8 in × 21 in.) |
| Weight | 24.5 kg (54 lb) |
| Power Requirements | 100–240 V ac, 50–60 Hz, autoranging |
| Operating Temperature | 4–40 °C (40–104 °F); cold-room-compatible (4 °C) as long as system power remains on |
| Operating Humidity Range | 5–95% relative, non-condensing |
| Leak Detection | Built-in, optical sensor |